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Title: | Synthesis and Characterization of Two 3,4-Dihydropyrimidinone Derivatives |
Authors: | Noor Raisan Ali Mahmood Shakir Magtoof |
Keywords: | 3,4- Dihydropyrimidine-2-(1H)-ones, Biginilli reaction. |
Issue Date: | 2018 |
Publisher: | university of Diyala |
Citation: | http://dx.doi.org/10.24237/djps.1404.463B |
Abstract: | In this study we have successfully synthesis and characterization two of [3,4-dihydropyrimidin-2-(1H) ones] (1a and 1b). The compounds were synthesized by reaction of ethyl acetoacetate and aromatic aldehyde with urea in the presence of ethanol and FeCl3.6H2O with 3-5 drops of HCl at 60-65 OC. Spectral measurements (e.g. FT-IR,1H-NMR and 13C-NMR) are used to investigate the chemical structures and characterize the obtained product of synthesized compounds. |
URI: | http://148.72.244.84:8080/xmlui/handle/xmlui/4793 |
ISSN: | 2222-8373 |
Appears in Collections: | مجلة ديالى للعلوم الاكاديمية / Academic Science Journal (Acad. Sci. J.) |
Files in This Item:
File | Description | Size | Format | |
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13e-P1(463).pdf | 298.09 kB | Adobe PDF | View/Open |
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