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http://148.72.244.84/xmlui/handle/xmlui/6289Full metadata record
| DC Field | Value | Language |
|---|---|---|
| dc.contributor.author | Luma Salman Abd | - |
| dc.date.accessioned | 2023-10-23T07:05:38Z | - |
| dc.date.available | 2023-10-23T07:05:38Z | - |
| dc.date.issued | 2016 | - |
| dc.identifier.issn | 2222-8373 | - |
| dc.identifier.uri | http://148.72.244.84:8080/xmlui/handle/xmlui/6289 | - |
| dc.description.abstract | In this research the preparation of target compound was completed in three sequential steps. Starting from furfural alcohol (1) that was converted to racemic 4-hydroxycyclopent-2-enone (2) in 39% yield after treated with catalytic amount of KH2PO4 in water as a solvent. Protection of the free hydroxyl group in (2) with t-butyldimethylsilyl chloride in the presence of DMAP was the next step to furnish compound (3) in yield of 50%. Organocuprate conjugate addition on (3) provide compound (4) in yield of 50%. | en_US |
| dc.description.sponsorship | https://djps.uodiyala.edu.iq/ | en_US |
| dc.language.iso | en | en_US |
| dc.publisher | University of Diyala | en_US |
| dc.subject | Key words: furfural alcohol, isopropyl group, dimethyl amine pyridine, conjugated addition | en_US |
| dc.title | Synthesis of-3-(tert-butyldimethylsilyoxy)-4-Isopropylcyclopentanone (4) | en_US |
| dc.title.alternative | تحضير وتشخيص المركب 3-(tert-butyldimethylsilyoxy)-4-isopropylcyclopentanone (4) | en_US |
| dc.type | Article | en_US |
| Appears in Collections: | مجلة ديالى للعلوم الاكاديمية / Academic Science Journal (Acad. Sci. J.) | |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| 28-40 E.pdf | 1.03 MB | Adobe PDF | View/Open |
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